Chemical Constants and Absolute Entropy by Rodebush W. H.

By Rodebush W. H.

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Enantiomeric Separation with Chiral Columns . . . . NMR Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72 72 73 73 75 78 81 83 83 85 87 4 Applications of Synthetic Pheromones for Pest Control . . . . . 88 References . . . . . . . . . . . . . . . . . . . . 91 . . . . . . . . . . . . . . . . . . . . . . . . . . . . Abstract As a consequence of the diversity of Lepidoptera, including 150,000 described species, interesting species-specific sex pheromone systems are exhibited in this insect group.

Starting from (S)-linalool [86]. An improved synthesis of (S)-39 by Mori is shown in Scheme 57 [87]. Enzymatic acetylation of (±)-2,3-epoxynerol (A) with vinyl acetate and lipase PS gave B together with C. The acetate B was converted to a multi-gram quantity of (S)-39 according to Oliver [86]. 05,9]dec-3-en-2-one (40) with unknown absolute configuration was isolated as a putative male pheromone of a Brazilian predatory stink bug (Tynacantha marginata), and its enantiomers were synthesized by Kuwahara as shown in Scheme 58 [88].

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